HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Hydroxide → Tetrabutylammonium diethylphosphate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| Reactant | Diethyl phosphoric acid | HCID 5166299 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water | HCID 962 | — |
| Product | Tetrabutylammonium diethylphosphate | HCID 87701958 | — |
Reaction Steps
12.8 ml of tetra-n-butylammonium hydroxide (20% solution in water) is dissolved in 20 ml of water, and 1 g of diethyl phosphate (75%), dissolved in 2 ml of acetone, is added dropwise with stirring and ice-cooling. The solution obtained is lyophilised.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08791129B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-db3b274457b740318a7b11d0337a574c |
| Source note | uspto-grants-2014_07 |