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HRID1631183

反应详情

EQUATION

反应方程式

HRID 1631183 的结构方程式

REACTANTS

反应物

2
结构：CCCC[N+](CCCC)(CCCC)CCCC.[OH-]
HCID2723671

Tetrabutylammonium Hydroxide

C16H37NO

结构：CCOP(=O)([O-])OCC
HCID5166299

Diethyl phosphate

C4H10O4P-

PRODUCTS

生成物

1
结构：CCCC[N+](CCCC)(CCCC)CCCC.CCOP(=O)([O-])OCC
HCID87701958

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

12.8 ml of tetra-n-butylammonium hydroxide (20% solution in water) is dissolved in 20 ml of water, and 1 g of diethyl phosphate (75%), dissolved in 2 ml of acetone, is added dropwise with stirring and ice-cooling. The solution obtained is lyophilised.

WORKUP

后处理

  1. additionis added dropwise
  2. temperatureice-cooling
  3. customThe solution obtained