HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 66886318, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | HCID 66853957 | HCID 66853957 | — |
| Product | HCID 66886318 | HCID 66886318 | 55% |
Reaction Steps
Prepared by the method described in Example 76, Step F using (R)-5-(2-(5-fluoro-2-(2-methoxyethoxy)phenyl)pyrrolidin-1-yl)pyrazolo[1,5-a]pyrimidine-3-carboxylic acid and ammonium chloride to yield the title compound as a white solid (32.6 mg, 55% yield). MS (apci) m/z=400.1 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08791123B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-068d12f294044d9fad1af30c62c443cc |
| Source note | uspto-grants-2014_07 |