反应详情

A sample of 23B (0.070 g, 0.31 mmol) was dissolved in 2 mL of 4M HCl in dioxane and stirred 1.5 h. The reaction was concentrated under reduced pressure to afford 23C.HCl (51 mg, quantitative yield) as a white solid. This material was used without characterization in the subsequent step.

1. concentrationThe reaction was concentrated under reduced pressure