Triethylamine → HCID 66707400, compound

Participants

Reaction Steps

To a solution of [4-(4-trifluoromethyl-phenoxymethyl)-phenyl]-methanol (intermediate 14.1.2, 0.34 g, 1.2 mmol) in dichloromethane (10 mL) were added triethylamine (0.34 mL, 2.4 mmol) and methanesulfonyl chloride (0.19 mL, 2.4 mmol). The reaction mixture was stirred at room temperature for 36 h under nitrogen atmosphere. The reaction mixture was washed with water, the organic layer was dried over MgSO4 and the solvent was evaporated under reduced pressure.

Provenance & Evidence