HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 4-Methoxyphenyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 4-Methoxyphenyl acetate | HCID 70987 | 103.5% |
Reaction Steps
A mixture of 4-methoxyphenol (6.2 g, 50 mmol), K2CO3 (10 g, 72 mmol) and acetic anhydride (6.12 g, 60 mmol) in acetone (150 ml) was stirred at RT. over night. The solid was filtered off and washed with acetone (50 ml). After removal of acetone, 8.6 g of product was obtained. Yield: 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08791267B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-407483a6e3744d34895315954d60d086 |
| Source note | uspto-grants-2014_07 |