HRID1632052

反应详情

EQUATION

反应方程式

HRID 1632052 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 4-methoxyphenol (6.2 g, 50 mmol), K2CO3 (10 g, 72 mmol) and acetic anhydride (6.12 g, 60 mmol) in acetone (150 ml) was stirred at RT. over night. The solid was filtered off and washed with acetone (50 ml). After removal of acetone, 8.6 g of product was obtained. Yield: 100%.

WORKUP

后处理

  1. waitover night
  2. filtrationThe solid was filtered off
  3. washwashed with acetone (50 ml)
  4. customAfter removal of acetone