HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20443325, compound → HCID 13339633, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20443325 | HCID 20443325 | — |
| Catalyst | Cuprous chloride | HCID 62652 | — |
| Solvent | 1,2-Dichlorobenzene | HCID 7239 | — |
| Product | HCID 13339633 | HCID 13339633 | 38% |
Reaction Steps
A slurry of 15 g (0.039 mole) of 3,6-dichloro-2-(1-bromo-3,3,3-trichloro-1-methylpropyl)pyridine and 5 g of finely divided CuCl in O-dichlorobenzene was washed at reflux for two hours. The mixture was cooled, filtered and the filtrate concentrated in vacuo. Recrystallization from pentane yielded 4.5 g (38%) of product, m.p. 71°-74° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04474602 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-177dcd539e17406c8b48b8e268fc3d1e |
| Source note | uspto-grants-1984_10 |