HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 20443861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 20443860 | HCID 20443860 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20443861 | HCID 20443861 | — |
Reaction Steps
Add 23.1 gm of 2-chloro-4,6-dihydro-3H[2]benzopyrano[3,4-b]pyridin-3-one to 100 ml of 40% aqueous methylamine and 250 ml of water. Heat the system in a steel bomb at 140° C. for 5 days. Stop the reaction and isolate the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04474786 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-de0707668e8a4000b343cdfc8aaef473 |
| Source note | uspto-grants-1984_10 |