Methylamine → HCID 20443861, compound

HRID 1632184Notes

Reaction equation

HRID 1632184 reaction equation
Cl[C:2]1[C:7](=[O:8])[NH:6][C:5]2[O:9][CH2:10][C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=3[C:4]=2[CH:3]=1.[CH3:17][NH2:18]>O>[CH3:17][NH:18][C:2]1[C:7](=[O:8])[NH:6][C:5]2[O:9][CH2:10][C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=3[C:4]=2[CH:3]=1

Participants

4

Reactant 2

HCID 6329MethylamineHCID 20443860HCID 20443860, compound

Product 1

HCID 20443861HCID 20443861, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Add 23.1 gm of 2-chloro-4,6-dihydro-3H[2]benzopyrano[3,4-b]pyridin-3-one to 100 ml of 40% aqueous methylamine and 250 ml of water. Heat the system in a steel bomb at 140° C. for 5 days. Stop the reaction and isolate the title compound.

Workup

  1. customthe reaction

Sources & evidence

ORD record
ord-de0707668e8a4000b343cdfc8aaef473
Source dataset
uspto-grants-1984_10
Patent number
US04474786

Reaction notes

Loading…