HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 20443831, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 20443860 | HCID 20443860 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20443831 | HCID 20443831 | — |
Reaction Steps
Add 23.1 gm of 2-chloro-4,6-dihydro-3H[2]benzopyrano[3,4-b]pyridin-3-one to 300 ml of methanol containing 30 gm of sodium methoxide. Heat the system in a steel bomb at about 200° C. for 12 hours. Stop the reaction and remove the solvent by stripping. Treat the residue with water and then isolate the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04474786 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-52ea9c7552af4cb7bbd58f53d918509f |
| Source note | uspto-grants-1984_10 |