HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 70511433, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2-(Octylamino)-1-{4-[(propan-2-yl)sulfanyl]phenyl}butan-1-ol--hydrogen chloride (1/1) | HCID 3042893 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 70511433 | HCID 70511433 | — |
Reaction Steps
To 20 ml of acetonitrile, 5 gr (13 mmol) of 1-(4-isopropylthiophenyl)-2-n-octylamino-1-butanol hydrochloride and 5.3 g (52 mmol) of acetic anhydride are added successively. The mixture is refluxed for 2.5 hours. When cooling, it abandons a white solid. The latter is filtered off and twice recrystallised from acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04474977 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-a0deff82a0fb43e690c69b93645822ea |
| Source note | uspto-grants-1984_10 |