HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → H-Leu-Leu-Ala-Gln-OH
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Z-Leu-Leu-Ala-Gln-OH | HCID 131713838 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | H-Leu-Leu-Ala-Gln-OH | HCID 131713837 | — |
Reaction Steps
To 1.50 g of Z-Leu-Leu-Ala-Gln-OH was added 20 ml of acetic acid containing 25% of hydrogen bromide, then the mixture was stirred at a room temperature for 1 hour. To the reaction mixture was added dried ether, and solid material precipitated was collected by filtration to obtain H-Leu-Leu-Ala-Gln-OH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04474754 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-2a8709566dd247ba85ebf9e2659fa3ec |
| Source note | uspto-grants-1984_10 |