Hydrochloric Acid → H-Leu-Gly-Oet

HRID 1632393Notes

Reaction equation

HRID 1632393 reaction equation
[NH:1](C(OCC1C=CC=CC=1)=O)[C@H:2]([C:7]([NH:9][CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12])=[O:8])[CH2:3][CH:4]([CH3:6])[CH3:5].Cl>CO.[Pd]>[NH2:1][C@H:2]([C:7]([NH:9][CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12])=[O:8])[CH2:3][CH:4]([CH3:5])[CH3:6]

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 11810251Z-Leu-Gly-OEt

Product 1

HCID 11390304H-Leu-Gly-Oet

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

3.12 Grams of Z-Leu-Gly-OC2H5 was dissolved in 50 ml of methanol and 8.90 ml of 1N hydrochloric acid and the solution was catalytically reduced by using palladium as the catalyst to obtain H-Leu-Gly-OC2H5.

Sources & evidence

ORD record
ord-6a58f1f676ab4aceb9d43b1185581192
Source dataset
uspto-grants-1984_10
Patent number
US04474754

Reaction notes

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