HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13150642, compound → HCID 131713868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13150642 | HCID 13150642 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131713868 | HCID 131713868 | — |
Reaction Steps
2.79 Grams of Z-Leu-Gln-NHNHBoc was suspended in 80 ml of methanol, a small amount of palladium black was added to this suspension and the suspension was stirred for 32 hours under the condition of introducing hydrogen gas. After completion of the reaction, the catalyst was removed by suction filtration, the filtrate was subjected to distillation under a reduced pressure, the residue obtained was dried under a reduced pressure in a desiccator to obtain the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04474754 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-83d551683030454d9fa938df546b84c4 |
| Source note | uspto-grants-1984_10 |