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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1632413Generated: October 29, 2026

HCID 13150642, compound → HCID 131713868, compound

https://huagongshe.com/reaction/1632413

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 13150642HCID 13150642—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 131713868HCID 131713868—

Reaction Steps

2.79 Grams of Z-Leu-Gln-NHNHBoc was suspended in 80 ml of methanol, a small amount of palladium black was added to this suspension and the suspension was stirred for 32 hours under the condition of introducing hydrogen gas. After completion of the reaction, the catalyst was removed by suction filtration, the filtrate was subjected to distillation under a reduced pressure, the residue obtained was dried under a reduced pressure in a desiccator to obtain the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04474754
Source datasetuspto-grants-1984_10
ORD IDord-83d551683030454d9fa938df546b84c4
Source noteuspto-grants-1984_10