Hydrogen Peroxide → HCID 20210490, compound

HRID 1632736Notes

Reaction equation

HRID 1632736 reaction equation
[OH:1]O.[CH2:3]([S:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[NH:13][C:14]3[C:19]([N:20]=2)=[CH:18][N:17]=[N:16][CH:15]=3)=[C:8]([O:21][CH3:22])[CH:7]=1)[CH3:4]>C(O)C>[CH2:3]([S:5]([C:6]1[CH:11]=[CH:10][C:9]([C:12]2[NH:20][C:19]3[C:14]([N:13]=2)=[CH:15][N:16]=[N:17][CH:18]=3)=[C:8]([O:21][CH3:22])[CH:7]=1)=[O:1])[CH3:4]

Participants

4

Reactant 2

HCID 784Hydrogen PeroxideHCID 132324742-[4-(Ethylsulfanyl)-2-methoxyphenyl]-1H-imidazo[4,5-d]pyridazine

Product 1

HCID 20210490HCID 20210490, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

10 ml of 30% strength H2O2 are added to a boiling solution of 2.84 g of 2-(4-ethylthio-2-methoxyphenyl)-1,3,5,6-tetraazaindene in 50 ml of ethanol, and the mixture is then boiled for 3 hours. Cooling down and customary working up gives 2-(4-ethylsulfinyl-2-methoxyphenyl)-1,3,5,6-tetraazaindene.

Workup

  1. temperatureCooling down and

Sources & evidence

ORD record
ord-46658899668144d9aa7e3cf4b2b3ee2b
Source dataset
uspto-grants-1984_10
Patent number
US04477454

Reaction notes

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