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HRID1632738

反应详情

EQUATION

反应方程式

HRID 1632738 的结构方程式

REACTANTS

反应物

1
结构：CN(C)CC(C)(C)C(=O)O.Cl
HCID86179916

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)CC(C)(C)C(=O)Cl.Cl
HCID20442369

3-(Dimethylamino)-2,2-dimethylpropanoyl chloride--hydrogen chloride (1/1)

C7H15Cl2NO

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O=S(Cl)Cl
溶剂HCID24386

Thionyl chloride

Cl2OS

PROCEDURE

实验过程

A mixture of 2,2-dimethyl-3-dimethylaminopropionic acid hydrochloride (1.76 g, 0.00969 mole) and thionyl chloride (10 ml) was heated under reflux for 30 minutes.

WORKUP

后处理

  1. temperaturewas heated
  2. temperatureunder reflux for 30 minutes