Acetone → HCID 70463992, compound

HRID 1632781Notes

Reaction equation

HRID 1632781 reaction equation
[CH3:1][C:2]1[C:8]([OH:9])=[CH:7][CH:6]=[CH:5][C:3]=1[OH:4].[CH3:10][C:11]([CH3:13])=[O:12]>P(Cl)(Cl)(Cl)=O.O>[CH3:1][C:2]1[C:8]([OH:9])=[CH:7][CH:6]=[CH:5][C:3]=1[OH:4].[CH3:10][C:11]([CH3:13])=[O:12]

Participants

5

Reactant 2

HCID 180AcetoneHCID 118432-Methylresorcinol

Product 1

HCID 70463992HCID 70463992, compound

Reagents, catalysts & solvents 2

HCID 24813Phosphorus oxychlorideCatalystHCID 962WaterSolvent

Procedure

To a solution of 621 g. of 2-methylresorcinol in 1 l. of acetone were added 30 g. of phosphorus oxychloride as a catalyst and the resulting mixture was stirred at room temperature for 24 hours. After completion of the reaction, the reaction mixture was poured into 10 l. of a cold water to give a pale brown powdery resin.

Workup

  1. customAfter completion of the reaction
  2. additionthe reaction mixture was poured into 10 l

Sources & evidence

ORD record
ord-2ac19e485776498e9ca93045a698e877
Source dataset
uspto-grants-1984_10
Patent number
US04477553

Reaction notes

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