HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → HCID 178447908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 178447910 | HCID 178447910 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178447908 | HCID 178447908 | — |
Reaction Steps
A mixture of 28.9 g of 2-ethoxy-5-(trans-4-propyl-cyclohexyl)-benzaldoxime (obtainable from the aldehyde and hydroxylamine) and 40 ml of acetic anhydride is heated until the exothermic reaction starts, and is then boiled for 20 minutes and poured into water to give 2-ethoxy-5-(trans-4-propyl-cyclohexyl)-benzonitrile of m.p. 32°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04478740 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-e269fb783078497a82485d82d963fc4e |
| Source note | uspto-grants-1984_10 |