HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethyl isocyanate → HCID 20441648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethyl isocyanate | HCID 16035 | — |
| Reactant | 5-Chloro-2(1H)-pyrimidinone | HCID 108578 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20441648 | HCID 20441648 | 40% |
Reaction Steps
was prepared from 5-chloropyrimidin-2-one and 2-chloroethylisocyanate in dimethyl formamide as described above; yield 40%. 1H NMR (DMSO-d6): δ3.6 (CH2CH2, broad m), 8.41 (2H-4,6), 9.5 (NH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04478839 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-c0c07141414549dd840de6b8088f5d0a |
| Source note | uspto-grants-1984_10 |