Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 1-(3,4,5-Trimethoxycinnamoyl)-4-[1-(isopropylaminocarbonyl)ethyl]piperazine Hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 1-(3,4,5-Trimethoxycinnamoyl)-4-[1-(isopropylaminocarbonyl)ethyl]piperazin | HCID 54378678 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-(3,4,5-Trimethoxycinnamoyl)-4-[1-(isopropylaminocarbonyl)ethyl]piperazine Hydrochloride | HCID 70505558 | — |
반응 단계
3 ml of 15% ethanolic hydrogenchloride is added to a solution of 3.00 g of 1-(3,4,5-trimethoxycinnamoyl)-4-[1-(isopropylaminocarbonyl)ethyl]piperazine prepared as in Example 3 in 5 ml of ethanol, and the solvent is distilled off. Isopropanol is added to the abtained residue and the precipitates are collected by filtration.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04478838 |
| 출처 데이터셋 | uspto-grants-1984_10 |
| ORD ID | ord-50125aaf1ec94dc5bcf46cee6f194dd8 |
| 출처 메모 | uspto-grants-1984_10 |