HRID1633032

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8016

N-Methyl-N-hydroxyethylamine

C3H9NO

结构：O=S1CCN(c2nc(Cl)nc3c(NCc4ccccc4)ncnc23)CC1

HCID12817012

未命名化合物

PRODUCTS

生成物

结构：CN(CCO)c1nc(N2CCS(=O)CC2)c2ncnc(NCc3ccccc3)c2n1

HCID54324454

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

This compound was prepared analogous to Example 2 from 8-benzylamino-2-chloro-4-(1-oxido-thiomorpholino)pyrimido[5,4-d]pyrimidine (melting point: 232°-233° C.) and N-(2-hydroxy-ethyl)-methylamine in dioxane under reflux.

WORKUP

后处理

temperatureunder reflux