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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1633032Generated: October 26, 2026

2-(Methylamino)ethanol → HCID 54324454, compound

https://huagongshe.com/reaction/1633032

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-(Methylamino)ethanolHCID 8016—
Reactant8-Benzylamino-2-chloro-4-(1-oxido-thiomorpholino)pyrimido[5,4-d]pyrimidineHCID 12817012—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 54324454HCID 54324454—

Reaction Steps

This compound was prepared analogous to Example 2 from 8-benzylamino-2-chloro-4-(1-oxido-thiomorpholino)pyrimido[5,4-d]pyrimidine (melting point: 232°-233° C.) and N-(2-hydroxy-ethyl)-methylamine in dioxane under reflux.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04478833
Source datasetuspto-grants-1984_10
ORD IDord-67e90d6a94a1472aa5869ecd2db78bc4
Source noteuspto-grants-1984_10