Hydrazine hydrate (1:1) → HCID 12582745, compound

HRID 1633033Notes

Reaction equation

HRID 1633033 reaction equation
Cl[C:2]1[N:7]=[N:6][C:5]2[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][C:4]=2[CH:3]=1.O.[NH2:15][NH2:16]>>[NH:15]([C:2]1[N:7]=[N:6][C:5]2[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][C:4]=2[CH:3]=1)[NH2:16]

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 20441588HCID 20441588, compound

Product 1

HCID 12582745HCID 12582745, compound

Procedure

11.7 g of 3-chloro-5,6,7,8,9,10-hexahydrocycloocta[c]pyridazine and 60 cc of hydrazine hydrate are reacted in accordance with the process described in Example 1. The orange-coloured solution is completely concentrated, and the remaining crystalline crude title compound is washed with water. M.P. 145°-145° (decomp., from absolute ethanol).

Workup

  1. concentrationThe orange-coloured solution is completely concentrated
  2. washthe remaining crystalline crude title compound is washed with water

Sources & evidence

ORD record
ord-f5bd0693cd324505b4f6f8cd167791b5
Source dataset
uspto-grants-1984_10
Patent number
US04478837

Reaction notes

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