反应详情

A solution of 4 g of 1-(7-methoxycarbonylheptyl)-3-methyl-2-(3-pyridyl)indole in 40 ml of n-butanol is saturated with methylamine and heated on a steam bath in a pressure bottle for 3 days. The reaction mixture is evaporated to dryness and the product is crystallized from ethyl-ether to yield the 1-[7-(N-methylcarbamoyl)heptyl]-3-methyl-2-(3-pyridyl)indole.

1. temperatureheated on a steam bath in a pressure bottle for 3 days
2. customThe reaction mixture is evaporated to dryness
3. customthe product is crystallized from ethyl-ether