HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20439642, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 20439640 | HCID 20439640 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20439642 | HCID 20439642 | 75.9% |
Reaction Steps
An amount of 4.5 gm of 2-chloro-3-(4-chlorophenoxy)-6-nitro-N-2-hydroxyethylaniline was dissolved in 40 ml of toluene and mixed with 2.9 gm of PCl5, spontaneous heating and gas generation taking place. After 30 minutes the mixture was shaken with water and sodium bicarbonate solution and is evaporated. 3.6 gm of a yellowy brown oil were obtained (76% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE031717 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-fe2ea5881bec472c9b2a80fd8bc2e4bc |
| Source note | uspto-grants-1984_10 |