Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | Cyanamide | HCID 9864 | — |
| Product | HCID 20440090 | HCID 20440090 | — |
Reaction Steps
64% Hydrazine solution (50 g, 1 mole) and 70% nitric acid (45 g, 0.5 mole) were carefully mixed in 200 ml of ethanol. 50% Aqueous cyanamide solution (42 g, 0.5 mole) was added and the mixture refluxed two hours. The solution was cooled to 20° C. precipitating the product which was then recrystallized from methanol giving 15 g of white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04479917 |
|---|
| Source dataset | uspto-grants-1984_10 |
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| ORD ID | ord-fb135aa95d3441818523b457770b4e96 |
|---|
| Source note | uspto-grants-1984_10 |
|---|
