HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → o-nitrobenzenesulfenamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 2-Nitrobenzenesulfenyl chloride | HCID 24319 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | o-nitrobenzenesulfenamide | HCID 350641 | — |
Reaction Steps
50 grams of o-nitrobenzenesulfenyl chloride was added to carbon tetrachloride with stirring, followed by 50 milliliters of ammonium hydroxide over a one-minute period. The stirring was continued over 5 minutes to obtain an o-nitrobenzenesulfenamide intermediate which precipitated in the reaction mixture. The o-nitrobenzenesulfenamide intermediate was recovered by filtration and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04479953 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-060deb2f1e804478a5a7e0f67e863868 |
| Source note | uspto-grants-1984_10 |