HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → Hydrogen Peroxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Cyclohexanol | HCID 7966 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Hydrogen Peroxide | HCID 784 | 90% |
| Product | Cyclohexanone | HCID 7967 | — |
Reaction Steps
50 cc of methanol (40 g), 20 g of cyclohexanol, 6 cc of 36% w/v aqueous hydrogen peroxide and 3 g of catalyst are fed into a glass autoclave. After 4 hours at 88° C., 95.6% of the fed hydrogen peroxide has reacted. 5.6 g of cyclohexanone are obtained with an H2O2 yield of 90%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04480135 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-7e9dd09177db4c8f9bb004870d6ec04d |
| Source note | uspto-grants-1984_10 |