1,4-Butanediol → HCID 86739745, compound
Reaction equation
[CH:1](=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:14]([OH:19])[CH2:15][CH2:16][CH2:17][OH:18]>CC(C)=O>[CH2:14]([OH:19])[CH2:15][CH2:16][CH2:17][OH:18].[CH:1](=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 50 °C
Procedure
Dodecanal (5 g) was reacted with 1,4-butane diol (1 g) by warming the mixture to 50° C. in order to melt the dodecanal and then allowing it to cool to room temperature. The mixture went completely solid and was worked up as in Example 3 with acetone to yield the 1,4-butane diol/dodecanal adduct (1.1 g) M.Pt. 51° C.
Workup
- temperatureto cool to room temperature
Sources & evidence
- ORD record
- ord-1436733211fe475e867f2841535cc2af
- Source dataset
- uspto-grants-1984_10
- Patent number
- US04480139
Reaction notes
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