Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,4-Butanediol | HCID 8064 | — |
| Reactant | Dodecanal | HCID 8194 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86739745 | HCID 86739745 | 36.1% |
Reaction Steps
Dodecanal (5 g) was reacted with 1,4-butane diol (1 g) by warming the mixture to 50° C. in order to melt the dodecanal and then allowing it to cool to room temperature. The mixture went completely solid and was worked up as in Example 3 with acetone to yield the 1,4-butane diol/dodecanal adduct (1.1 g) M.Pt. 51° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04480139 |
|---|
| Source dataset | uspto-grants-1984_10 |
|---|
| ORD ID | ord-1436733211fe475e867f2841535cc2af |
|---|
| Source note | uspto-grants-1984_10 |
|---|
