Diethylamine → HCID 18679561, compound
Reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][O:8][C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[N:14]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[CH:13]=[CH:12]2.[CH2:24]([NH:26][CH2:27][CH3:28])[CH3:25]>>[CH2:24]([N:26]([CH2:27][CH3:28])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][O:8][C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[N:14]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[CH:13]=[CH:12]2)[CH3:25]Participants
3
Procedure
In analogy to example 4.4, 5-(6-Bromo-hexyloxy)-1-phenyl-1H-indole and diethylamine were converted to yield Diethyl-[6-(1-phenyl-1H-indol-5-yloxy)-hexyl]-amine as colorless oil, MS: 365 (MH+).
Sources & evidence
- ORD record
- ord-68be2ad3f76f474da073f83e9fe46ba0
- Source dataset
- uspto-grants-2003_01
- Patent number
- US06503907B2
Reaction notes
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