참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | HCID 54098056 | HCID 54098056 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | Octyl-sepharose CL-4B | HCID 112041 | 100% |
반응 단계
In a 500-mL autoclave were added 100 g of the resulting octadienyl glyceryl ether and 5 g of 5% Pd—C (product of NE Chemcat Corporation). The mixture was stirred at 25 to 70° C. for 6 hours under a hydrogen atmosphere of 1 to 5 MPa. After completion of the reaction, the catalyst was filtered away, whereby 102 g of octyl glyceryl ether was obtained as a colorless transparent oil. GC analysis of the resulting oil showed that the content of monooctyl glyceryl ether was 99%, while that of dioctyl glyceryl ether was 1% or less.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06504063B2 |
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| 출처 데이터셋 | uspto-grants-2003_01 |
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| ORD ID | ord-6e8d08cd7fac4c00bb714f15823ecb07 |
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| 출처 메모 | uspto-grants-2003_01 |
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