反应详情

温度

47.5 °C

In a 500-mL autoclave were added 100 g of the resulting octadienyl glyceryl ether and 5 g of 5% Pd—C (product of NE Chemcat Corporation). The mixture was stirred at 25 to 70° C. for 6 hours under a hydrogen atmosphere of 1 to 5 MPa. After completion of the reaction, the catalyst was filtered away, whereby 102 g of octyl glyceryl ether was obtained as a colorless transparent oil. GC analysis of the resulting oil showed that the content of monooctyl glyceryl ether was 99%, while that of dioctyl glyceryl ether was 1% or less.

1. customAfter completion of the reaction
2. filtrationthe catalyst was filtered away