HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 18680072, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 18680150 | HCID 18680150 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 18680072 | HCID 18680072 | — |
Reaction Steps
A solution of Example 20A (240 mg, 0.66 mmol), ethyl iodide (0.11 mL, 1.32 mmol), and triethylamine (0.18 mL, 1.32 mmol) in THF at 45° C. was stirred for 4 hours and concentrated. The concentrate was purified by flash column chromatography with 30% ethyl acetate/hexanes to provide the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06504031B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-954fecc41ae74fa2afb6489d12931728 |
| Source note | uspto-grants-2003_01 |