反应详情

The above resin bound acrylic acid (50 mg) was treated with 300 μmol cyclopropylmethyl amine (21.3 mg) in 300 μL DMSO for 72 hours at 25° C. The excess reagent was filtered off and the resin was washed with 3×1 mL DMSO and 3×1 mL DMF.

1. filtrationThe excess reagent was filtered off
2. washthe resin was washed with 3×1 mL DMSO and 3×1 mL DMF