HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylic Acid → N-(cyclopropylmethyl)-3-aminopropionic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Cyclopropanemethanamine | HCID 75646 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | N-(cyclopropylmethyl)-3-aminopropionic Acid | HCID 22502000 | — |
Reaction Steps
The above resin bound acrylic acid (50 mg) was treated with 300 μmol cyclopropylmethyl amine (21.3 mg) in 300 μL DMSO for 72 hours at 25° C. The excess reagent was filtered off and the resin was washed with 3×1 mL DMSO and 3×1 mL DMF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06503949B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-5ead5eb1ed214f5585852a2a6430bbb4 |
| Source note | uspto-grants-2003_01 |