HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl isocyanate → HCID 70000528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl isocyanate | HCID 76639 | — |
| Reactant | HCID 70001094 | HCID 70001094 | — |
| Product | HCID 70000528 | HCID 70000528 | — |
Reaction Steps
Treatment of 3-[2-(7-amino-5-oxo-2,3-dihydro-5H-benzo[f][1,4]oxazepin-4-yl)-acetylamino]-propionic acid ethyl ester (0.17 g, 0.5 mmol) with benzylisocyanate as described in Example 1 d) yielded 3-{2-[7-(3-benzyl-ureido)-5-oxo-2,3-dihydro-5H-benzo[f][1,4]oxazepin-4-yl]-acetylamino}-propionic acid ethyl ester (0.2 g, 0.42 mmol): mp. 70-75° C.; MS (ISP): 469 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506744B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-faf3736cf8f84e23a437846e327a31b5 |
| Source note | uspto-grants-2003_01 |