HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23552469, compound → Acetonitrile--water (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23552469 | HCID 23552469 | — |
| Reactant | HCID 178418255 | HCID 178418255 | — |
| Product | Acetonitrile--water (1/1) | HCID 18373917 | 37% |
| Product | HCID 18677493 | HCID 18677493 | — |
Reaction Steps
The title compound was prepared in accordance with the general method of example 371 from 2,6-bis-acetylamino-N-methoxy-N-methyl-isonicotinamide and phenylmagnesium bromide. The purification was performed by reversed phase HPLC eluting with an acetonitrile/water gradient Yield: 37%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506772B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-a78f7aa07087417ab98538e1221d1140 |
| Source note | uspto-grants-2003_01 |