HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromofuran-2-carbaldehyde → HCID 18677549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromofuran-2-carbaldehyde | HCID 600328 | — |
| Reactant | O-mesitylenesulfonylhydroxylamine | HCID 11009332 | — |
| Reactant | HCID 18677493 | HCID 18677493 | — |
| Product | HCID 18677549 | HCID 18677549 | — |
Reaction Steps
The title compound, MS m/e (%): 383 (M+H+, 100), was prepared in accordance with the general method of example 373 from (2,6-diamino-pyridin-4-yl)-phenyl-methanone, o-mesitylene-sulfonylhydroxylamine, and 5-bromo-2-furaldehyde. The purification was performed with reversed phase HPLC eluting with an acetonitrile/water gradient.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506772B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-5e9c55f1e9de433480488f722b182162 |
| Source note | uspto-grants-2003_01 |