HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pyridinecarboxaldehyde → HCID 18677525, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pyridinecarboxaldehyde | HCID 14273 | — |
| Reactant | O-mesitylenesulfonylhydroxylamine | HCID 11009332 | — |
| Reactant | HCID 18677493 | HCID 18677493 | — |
| Product | HCID 18677525 | HCID 18677525 | — |
Reaction Steps
The title compound, MS m/e (%): 316 (M+H+, 100), was prepared in accordance with the general method of example 373 from (2,6-diamino-pyridin-4-yl)-phenyl-methanone, o-mesitylene-sulfonylhydroxylamine, and pyridine-2-carbaldehyde. The purification was performed with reversed phase HPLC eluting with an acetonitrile/water gradient.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506772B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-1ba29f93e8284d2dba40cfb4fe26a2ca |
| Source note | uspto-grants-2003_01 |