HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 15450534, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 15450533 | HCID 15450533 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15450534 | HCID 15450534 | — |
Reaction Steps
A mixture of 1,349 mg of the above obtained 5-acetoxybenzo[b]thiophene-3-carboxylic acid (4), a drop of dimethylformamide, 1.22 ml of (17.13 mmol) of thionyl chloride and 25 ml of toluene was refluxed for 1.5 hours and then concentrated under reduced pressure to give 1,454 mg of the objective compound (5).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506789B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-b4374e36e5f6435bbbfe14f1c7db2aa0 |
| Source note | uspto-grants-2003_01 |