Aluminium lithium hydride → HCID 178477845, compound

Participants

Reaction Steps

To a solution of compound (16) (0.65 g; 1.5 mmol) in anhydrous tetrahydrofuran (70 ml) was added a 1.0M solution of lithium aluminum hydride in tetrahydrofuran (4.6 ml; 4.6 mmol). The mixture was stirred at room temperature for 1.75 h. then diluted with ethyl ether and quenched with dropwise addition of saturated ammonium chloride solution. To saturated ammonium chloride

Provenance & Evidence