HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Piperidinecarboxamide → HCID 18678470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Piperidinecarboxamide | HCID 3772 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1,1,1-Trifluoro-3-iodopropane | HCID 156165 | — |
| Product | HCID 18678470 | HCID 18678470 | 23.4% |
Reaction Steps
Prepared from isonipecotamide (2.85 g, 22.3 mmol), 3,3,3-trifluoropropyl iodide (5 g, 22.3 mmol) and potassium carbonate (3.08 g, 22.3 mmol) of according to the procedure used for Example 8 (Step A) to give 1.17 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506901B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-7a731ffcfcdd46eba37e816b0b9b6607 |
| Source note | uspto-grants-2003_01 |