HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18678470, compound → HCID 18678579, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18678470 | HCID 18678470 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 18678579 | HCID 18678579 | 96% |
Reaction Steps
Prepared from 1-(3,3,3-trifluoropropyl)-piperidine-4-carboxamide (1.0 g, 4.46 mmol) and LAH (0.34 g, 8.9 mmol) according to general the procedure used for Example 8 (Step B) to give 0.9 g of title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506901B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-230499c4f2c745a191b79e928228ff2e |
| Source note | uspto-grants-2003_01 |