HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Piperidinecarboxamide → HCID 18678407, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Piperidinecarboxamide | HCID 3772 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1,1,1-Trifluoro-4-iodobutane | HCID 2775189 | — |
| Product | HCID 18678407 | HCID 18678407 | 106.8% |
Reaction Steps
Prepared from isonipecotamide (0.422 g, 3.3 mmol), 4,4,4-trifluorobutyliodide (0.82 g, 3.4 mmol) and potassium carbonate (0.47 g, 3.4 mmol) according to the procedure used for Example 8 (Step A) to give 0.84 g of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506901B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-5b70c2deecd34d76863d6f0fa0c5e003 |
| Source note | uspto-grants-2003_01 |