HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18678407, compound → HCID 18678636, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18678407 | HCID 18678407 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 18678636 | HCID 18678636 | 98.6% |
Reaction Steps
Prepared from 1-(4,4,4-trifluorobutyl)-piperidine-4-carboxamide (0.82 g, 3.3 mmol) and LAH (0.25 g, 6.6 mmol) according to general the procedure used for Example 8 (Step B) to give 0.73 g of title compound as a clear oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506901B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-038861febb4446bdac6f449ad42c735a |
| Source note | uspto-grants-2003_01 |