HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 3297718, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | Octylamine | HCID 8143 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 3297718 | HCID 3297718 | 98.3% |
Reaction Steps
A solution of octyl amine (22.79 g, 176 mmol) and phenyl isocyanate (21 g, 176 mmol) in THF (200 ml) at 0° C. was stirred for 2 hours. The solvent was evaporated in vacuo and the residue was triturated with hexane to give 43 g of final product (173 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506901B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-60d621653d5746489f7203d49391a857 |
| Source note | uspto-grants-2003_01 |