HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 18678744, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | HCID 18678450 | HCID 18678450 | — |
| Reactant | CID 71317501 | HCID 71317501 | — |
| Product | HCID 18678744 | HCID 18678744 | — |
Reaction Steps
The title compound was prepared from 1-(2,6-difluoro-benzyl)-3-[4-(4-dimethoxymethyl-piperidine-1-sulfonyl)-phenyl]-1-methyl-urea (0.250 g, 0.5 mmol), sodium iodide (0.188 g, 1.26 mmol), and trichloromethylsilane (0.118 mL, 1.0 mmol) according to the procedure used for example 84 (Step D) and used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506901B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-8ca48cf9f5d347cfb59593a7cf865eaf |
| Source note | uspto-grants-2003_01 |