Diisopropylethylamine → HCID 59032956, compound

Participants

Role	Name	HCID	Charge
Reactant	Diisopropylethylamine	HCID 81531	—
Reactant	t-butyl-[4-(2S)-oxiranylmethoxy-phenoxy]-diphenylsilane	HCID 11327180	—
Reactant	HCID 86758801	HCID 86758801	—
Product	HCID 59032956	HCID 59032956	13.4%

Reaction Steps

Prepared from t-butyl-[4-(2S)-oxiranylmethoxy-phenoxy]-diphenylsilane (0.623 g, 1.54 mmol), (1H)-Indazole-3-carboxylic acid [4-(4-aminomethyl-1-piperidinyl-sulfonyl)-phenyl]-amide formate salt (0.71 g, xx mmol) and diisopropylethyl amine (0.41 mL) according to the procedure used for example 37 to give 0.12 g of the title compound as a white solid.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06506901B2
Source dataset	uspto-grants-2003_01
ORD ID	ord-1c8268de2e234750ac0c3a82980751ad
Source note	uspto-grants-2003_01